Rick Mathew
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I use the Alk...Ca...Phosphorous (converted to PO4) and Nitrite Checkers. With good lab testing methodology I have gotten very repeatable and reproducible results. It took a little work to get the test procedures nailed down but my gage R&R error is now less than 10% of the allowable limits of the test being performed. (Ex. Ca...350-450...Range 100...Gage error about 9) Therefore my test precision is good. I check the accuracy on a quarterly basis by comparing my results to outside testing results and for the most part my results are withing +- 10% of their results (Exception is PO4...Have some work to do here to get better accuracy, but the precision is good...always testing a bit high)
Just a note on the Hanna Calcium Checker. I have had very good success with this checker and have been using it for over 2 years. I made three changes that brought my Gage repeatability and reproducibility to less than 10% of the target range (100...350-450)
1) Purchased .3mL syringe...very accurate...You can find these from multiple suppliers
2) Use Hanna Deionized water (HI70436) and not my RODI water which has a small amount of calcium in it and is variable from batch to batch.
With the dilution ratio being so high and the water sample amount being so small these two changes took my R&R (repeatability and reproducibility) from between 30-40% (not good! almost random results) to less than 10% a very acceptable range for this test. My results have been validated by external testing sources so I feel confident in the measurement.
3) After the test is complete I rinse the vial and cap with the Hanna deionized water then fill the vial to the top with this water and store it this way until next use. Then on the next use I empty the vial do a quick rinse with the deionized water and proceed with the test.
IMO with good laboratory practices these checkers are great tools and do not rely on color change interpretation to make the measurement which in itself is a variable
Just a note on the Hanna Calcium Checker. I have had very good success with this checker and have been using it for over 2 years. I made three changes that brought my Gage repeatability and reproducibility to less than 10% of the target range (100...350-450)
1) Purchased .3mL syringe...very accurate...You can find these from multiple suppliers
2) Use Hanna Deionized water (HI70436) and not my RODI water which has a small amount of calcium in it and is variable from batch to batch.
With the dilution ratio being so high and the water sample amount being so small these two changes took my R&R (repeatability and reproducibility) from between 30-40% (not good! almost random results) to less than 10% a very acceptable range for this test. My results have been validated by external testing sources so I feel confident in the measurement.
3) After the test is complete I rinse the vial and cap with the Hanna deionized water then fill the vial to the top with this water and store it this way until next use. Then on the next use I empty the vial do a quick rinse with the deionized water and proceed with the test.
IMO with good laboratory practices these checkers are great tools and do not rely on color change interpretation to make the measurement which in itself is a variable
The easiest calcium test out there is the Salifert test. I get accurate results when compared between Red sea, Salifert and Hannah.

