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I cleaned and sterilized the test. Same results as before. I have only had this kit for a month. 3 tests performed with readable results before these last 3 failed tests so it seems to me the reagents are not the problem. I just verified that the vial, spoon and syringe being cleaned and sanitized prior to this tells me there is nothing wrong with my test kit.
I am wondering if maybe something in my water could effect the test. The tank is in it's 5th week of cycling. I recently added sand from brs and some chaeto and "reef lemonade" from LFS.
ThisMy conjecture: something contaminated the reagents. The only way to check my idea is to test some other water that contains nitrate.

