tuning calcium reactor

Mandrake

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i’m trying to measure my effluent all with Salifert
test kit but can’t get a reading (too high dkh ) for test kit to read, i have tried 2mil of effluent instead of 4 with 4 drops of kh1 and 2mil of effluent with 2 drops of kh 1 still no color change?
 
It may take more than 1ml (entire syringe) of the reagent. If the color hasn't changed after using the first syringe, then just refill it and add them together.
 

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